Controlled preparation of In2O3, InOOH and In(OH)3via a one-pot aqueous solvothermal route

Tingjiang Yan; Xuxu Wang; Jinlin Long; Huaxiang Lin; Rusheng Yuan; Wenxin Dai; Zhaohui Li; Xianzhi Fu

doi:10.1039/B809313J

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Controlled preparation of In₂O₃, InOOH and In(OH)₃via a one-pot aqueous solvothermal route†

Tingjiang Yan,^a Xuxu Wang,*^a Jinlin Long,^a Huaxiang Lin,^a Rusheng Yuan,^a Wenxin Dai,^a Zhaohui Li^a and Xianzhi Fu*^a

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* Corresponding authors

^a State Key Laboratory Breeding Base of Photocatalysis, Research Institute of Photocatalysis, Fuzhou University, P. R. China
E-mail: xwang@fzu.edu.cn, xzfu@fzu.edu.cn
Fax: +86 591 83738608
Tel: +86 591 83779251

Abstract

Pure cubic In₂O₃, orthorhombic InOOH and cubic In(OH)₃ nanocrystals were separately synthesized via a one-pot aqueous solvothermal route at low temperature by simply regulating the amount of water in the ternary system H₂O–DMF–In(NO₃)₃·4.5H₂O.

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Supplementary files

XRD pattern of In(OH)₃, Raman spectra, HRTEM and SAED of the as-synthesizedproducts PDF (1080K)

Article information

DOI: https://doi.org/10.1039/B809313J
Article type: Letter
Submitted: 03 Jun 2008
Accepted: 31 Jul 2008
First published: 12 Aug 2008

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New J. Chem., 2008,32, 1843-1846

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Controlled preparation of In₂O₃, InOOH and In(OH)₃via a one-pot aqueous solvothermal route

T. Yan, X. Wang, J. Long, H. Lin, R. Yuan, W. Dai, Z. Li and X. Fu, New J. Chem., 2008, 32, 1843 DOI: 10.1039/B809313J

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New Journal of Chemistry