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Abstract | Cited by

Syntheses of α,β-unsaturated γ-lactams are described that are based on ring-closing metathesis in combination with enantioselective Ir-catalysed allylic amination using N-Boc-N-(but-2-enoyl)-amine as a pronucleophile. As an example application, the synthesis of a Baclofen analogue is presented.

Graphical abstract: Synthesis of α,β-unsaturated γ-lactams via asymmetric iridium-catalysed allylic substitution

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