An efficient two-step annelation of functionalised orthoesters with trimethylsilyloxyfuran derivatives, which delivers suitably decorated bicyclo[3.n.0]lactones in high overall yields and with complete diastereocontrol of up to three contiguous stereocenters, is reported.
N. Maulide and I. E. Markó, Chem. Commun., 2006, 1200 DOI: 10.1039/B600677A
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