Issue 5, 2004
From the journal:

Journal of Analytical Atomic Spectrometry

Investigation of the sulfur speciation in petroleum products by capillary gas chromatography with ICP-collision cell-MS detection†

Brice Bouyssiere,*ab   Peter Leonhard,b   Daniel Pröfrock,b   Franck Baco,c   Clementina Lopez Garcia,c   Steve Wilburd  and  Andreas Prangeb  

* Corresponding authors

a CNRS UMR 5034, Hélioparc, 2, av. Pr. Angot, Pau, France
E-mail: brice.bouyssiere@univ-pau.fr

b GKSS-Research Centre, Institute of Coastal Research/Physical and Chemical Analysis, Max-Planck Strasse 1, Geesthacht, Germany

c Institut Français du Pétrole, CEDI René Navarre, Vernaison, France

d Agilent Technologies Inc., 3380 146th Place SE, Suite 300, Bellevue, Washington 98007, USA

Abstract

Recent regulations concerning the low-sulfur gasoline require analytical methods able to provide specific information on sulfur containing compounds present in petroleum products at the ng g−1 range. The on-line coupling of capillary GC with ICP-collision cell-MS was proposed for the speciation of sulfur in hydrocarbon matrices. The technique showed an absolute detection limit 0.5 pg for a 1 µL sample injected in the splitless mode which is about two orders of magnitude lower than the currently used techniques.

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Article information

DOI
https://doi.org/10.1039/B310449D
Article type
Technical Note
Submitted
28 Aug 2003
Accepted
02 Feb 2004
First published
19 Feb 2004

J. Anal. At. Spectrom., 2004,19, 700-702

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Investigation of the sulfur speciation in petroleum products by capillary gas chromatography with ICP-collision cell-MS detection

B. Bouyssiere, P. Leonhard, D. Pröfrock, F. Baco, C. Lopez Garcia, S. Wilbur and A. Prange, J. Anal. At. Spectrom., 2004, 19, 700 DOI: 10.1039/B310449D

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