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Issue 19, 2004
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New Pb–Pb bonds: syntheses and molecular structures of hexabiphenyldiplumbane and tri(trisbiphenylplumbyl)plumbate

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Abstract

Reaction of lead(II) chloride with biphenylmagnesium bromide yields Bp3Pb–PbBp3 and [(THF)3Mg(μ-Cl)3Mg(THF)3][Pb(PbBp3)3] (Bp = biphenyl), which, upon single crystal X-ray crystallographic analysis, reveals an interesting variation of Pb–Pb bond distances.

Graphical abstract: New Pb–Pb bonds: syntheses and molecular structures of hexabiphenyldiplumbane and tri(trisbiphenylplumbyl)plumbate

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Article information


Submitted
03 Jun 2004
Accepted
13 Jul 2004
First published
20 Aug 2004

Chem. Commun., 2004, 2224-2225
Article type
Communication

New Pb–Pb bonds: syntheses and molecular structures of hexabiphenyldiplumbane and tri(trisbiphenylplumbyl)plumbate

Y. Wang, B. Quillian, P. Wei, X. Yang and G. H. Robinson, Chem. Commun., 2004, 2224
DOI: 10.1039/B408860N

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