Issue 13, 2004
From the journal:

Chemical Communications

Synthesis and X-ray crystal structures of the first antimony and bismuth calixarene complexes†

Lihua Liu,a   Lev N. Zakharov,b   Arnold L. Rheingold*b  and  Tracy A. Hanna*a  

* Corresponding authors

a Department of Chemistry, Texas Christian University, Box 298860, Fort Worth, TX 76129, USA
E-mail: t.hanna@tcu.edu
Fax: +1 817-2575851

b Department of Chemistry & Biochemistry, University of California at San Diego, 9500 Gilman Dr, La Jolla, CA 92093, USA

Abstract

The reaction of the monosodium salt of p-tert-butylcalix[4]arene (ButC4) with 2 equivalents of SbCl3 provides ButC4(SbCl)2 and the first bismuth calixarene complex was prepared by treatment of p-tert-butylcalix[8]arene (ButC8) with Bi[N(SiMe3)2]3 in toluene.

Graphical abstract: Synthesis and X-ray crystal structures of the first antimony and bismuth calixarene complexes

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Article information

DOI
https://doi.org/10.1039/B404051A
Article type
Communication
Submitted
16 Mar 2004
Accepted
04 May 2004
First published
25 May 2004

Chem. Commun., 2004, 1472-1473

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Synthesis and X-ray crystal structures of the first antimony and bismuth calixarene complexes

L. Liu, L. N. Zakharov, A. L. Rheingold and T. A. Hanna, Chem. Commun., 2004, 1472 DOI: 10.1039/B404051A

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