Issue 3, 2003
From the journal:

Green Chemistry

Preparative and mechanistic studies of solvent-free Rap–Stoermer reactions

Kazuhiro Yoshizawa,a   Shinji Toyota,a   Fumio Toda*a  and  Ingeborg Csöregh*b  

* Corresponding authors

a Department of Chemistry, Faculty of Science, Okayama University of Science, 1-1 Ridai-cho, Okayama 700-0005, Japan
E-mail: toda@chem.ous.ac.jp
Fax: +81 86 256 9604
Tel: +81 86 256 9604

b Structural Chemistry, Arrhenius Laboratory, Stockholm University, S-106 91 Stockholm, Sweden
E-mail: ics@struc.su.se
Fax: +46 8 163118
Tel: +46 8 162385

Abstract

Solvent-free Rap–Stoermer reactions were found to very efficiently give products in almost quantitative yield by just washing the reaction mixture with water. The reaction mechanism has been clarified completely by continuous IR spectral monitoring and by isolation of two reaction intermediates.

Graphical abstract: Preparative and mechanistic studies of solvent-free Rap–Stoermer reactions

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Article information

DOI
https://doi.org/10.1039/B303802P
Article type
Paper
Submitted
04 Apr 2003
First published
16 May 2003

Green Chem., 2003,5, 353-356

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Preparative and mechanistic studies of solvent-free Rap–Stoermer reactions

K. Yoshizawa, S. Toyota, F. Toda and I. Csöregh, Green Chem., 2003, 5, 353 DOI: 10.1039/B303802P

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