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Issue 3, 2003
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Synthesis and characterization of highly ordered mesoporous thin films with –COOH terminated pore surfaces

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Abstract

Highly ordered mesoporous inorganic–organic hybrid thin films with covalently bonded carboxylic acid (–COOH) terminal groups on the pore surfaces were synthesized by evaporation induced self-assembly of tetraethoxysilane, organosilanes, and a nonionic surfactant followed by acid hydrolysis and characterized using transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, surface acoustic wave (SAW) based N2 sorption, and thermogravimetric analysis (TGA) techniques.

Graphical abstract: Synthesis and characterization of highly ordered mesoporous thin films with –COOH terminated pore surfaces

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Publication details

The article was received on 23 Oct 2002, accepted on 23 Dec 2002 and first published on 13 Jan 2003


Article type: Communication
DOI: 10.1039/B210377J
Chem. Commun., 2003, 370-371

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    Synthesis and characterization of highly ordered mesoporous thin films with –COOH terminated pore surfaces

    N. Liu, R. A. Assink and C. J. Brinker, Chem. Commun., 2003, 370
    DOI: 10.1039/B210377J

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