Issue 3, 2003
From the journal:

Chemical Communications

Synthesis and characterization of highly ordered mesoporous thin films with –COOH terminated pore surfaces

Nanguo Liu,a   Roger A. Assinkb  and  C. Jeffrey Brinker*ab  

* Corresponding authors

a Department of Chemical and Nuclear Engineering and Center for Micro-Engineered Materials, The University of New Mexico, Albuquerque, NM, USA

b Sandia National Laboratories, MS 1349, Albuquerque, NM, USA
E-mail: cjbrink@sandia.gov
Fax: 01-505-272-7336
Tel: 01-505-272-7627

Abstract

Highly ordered mesoporous inorganic–organic hybrid thin films with covalently bonded carboxylic acid (–COOH) terminal groups on the pore surfaces were synthesized by evaporation induced self-assembly of tetraethoxysilane, organosilanes, and a nonionic surfactant followed by acid hydrolysis and characterized using transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, surface acoustic wave (SAW) based N2 sorption, and thermogravimetric analysis (TGA) techniques.

Graphical abstract: Synthesis and characterization of highly ordered mesoporous thin films with –COOH terminated pore surfaces

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Article information

DOI
https://doi.org/10.1039/B210377J
Article type
Communication
Submitted
23 Oct 2002
Accepted
23 Dec 2002
First published
13 Jan 2003

Chem. Commun., 2003, 370-371

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Synthesis and characterization of highly ordered mesoporous thin films with –COOH terminated pore surfaces

N. Liu, R. A. Assink and C. J. Brinker, Chem. Commun., 2003, 370 DOI: 10.1039/B210377J

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