Issue 2, 2002
From the journal:

PhysChemComm

Two-dimensional correlation gel permeation chromatography (2D correlation GPC) study of the sol–gel polymerization of octyltriethoxysilane. HCl-concentration dependence

Kenichi Izawa,   Toshiaki Ogasawara,   Hideki Masuda,   Hirofumi Okabayashi,   Charmian J. O'Connor  and  Isao Noda  

Abstract

Two-dimensional correlation gel permeation chromatography (2D GPC) was used to elucidate intricate details of the initial ten minutes of the sol–gel transition of n-octyltriethoxysilane (OTES), catalysed by 0.5 and 2.0 M HCl·H 2 O. The results demonstrate that the features of 2D GPC correlation spectra directly reflect the dynamic variation of reactions or interactions present during the polymerization process.

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Article information

DOI
https://doi.org/10.1039/B107635C
Article type
Paper

PhysChemComm, 2002,5, 12-16

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Two-dimensional correlation gel permeation chromatography (2D correlation GPC) study of the sol–gel polymerization of octyltriethoxysilane. HCl-concentration dependence

K. Izawa, T. Ogasawara, H. Masuda, H. Okabayashi, C. J. O'Connor and I. Noda, PhysChemComm, 2002, 5, 12 DOI: 10.1039/B107635C

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