Issue 8, 2000
From the journal:

Journal of the Chemical Society, Perkin Transactions 1

The reaction of 3-nitropyridine with sulfite ions; a pathway to 2,5-disubstituted pyridines

Jan M. Bakke,a   Eli Ranes,a   Christian Rømmingb  and  Ingrid Sletvolda  

a Department of Chemistry, The Norwegian University of Science and Technology, Sem Sælandsvei 8, Trondheim, Norway

b Department of Chemistry, University of Oslo, Blindern, PO 1033, Oslo, Norway

Abstract

The reaction of 3-nitropyridine with an aqueous solution of sodium sulfite gave the disodium salt of 5-(N-sulfohydroxyamino)pyridine-2-sulfonic acid (2) which on treatment with an acidic ion exchange resin gave 5-hydroxyaminopyridine-2-sulfonic acid (3). The yield of 3 from 3-nitropyridine was 63%. The structures of the products were verified by X-ray analysis.

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Article information

DOI
https://doi.org/10.1039/A909875E
Article type
Paper
Submitted
13 Dec 1999
Accepted
15 Feb 2000
First published
29 Mar 2000

J. Chem. Soc., Perkin Trans. 1, 2000, 1241-1243

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The reaction of 3-nitropyridine with sulfite ions; a pathway to 2,5-disubstituted pyridines

J. M. Bakke, E. Ranes, C. Rømming and I. Sletvold, J. Chem. Soc., Perkin Trans. 1, 2000, 1241 DOI: 10.1039/A909875E

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