Issue 11, 1999

Preparation of (±)-[1,2-13C2]Abscisic Acid for Use as a Stable and Pure Internal Standard

Abstract

[1,2-13C2]ABA, which is designed as a stable and pure internal standard for GC/MS analysis, is synthesized through the Witting reaction of 1-hydroxy-4-keto-α-ionone with carbomethoxymethylenetriphenylphosphorane prepared from [1,2-13C2]bromoacetic acid followed by saponification of the product methyl [1,2-13C2]ABA.

Article information

Article type
Paper

J. Chem. Res. (S), 1999, 658-659

Preparation of (±)-[1,2-13C2]Abscisic Acid for Use as a Stable and Pure Internal Standard

T. Asami, K. Sekimata, J. Ming Wang, K. Yoneyama, Y. Takeuchi and S. Yoshida, J. Chem. Res. (S), 1999, 658 DOI: 10.1039/A904712C

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