A selective TOCSY experiment based on the recently described DPFGSE selective excitation sequence has been developed: it employs gradient purging pulses which result in excellent lineshapes free of antiphase dispersive components, and has proven useful in the identification of a number of impurities in a pharmaceutical intermediate.
G. J. Sharman, Chem. Commun., 1999, 1319 DOI: 10.1039/A902459J
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