The use of routine refocused-decoupled INEPT 29Si NMR spectroscopy, in the presence of the chiral lanthanide shift reagent Eu(tfc)3, allows convenient enantiomeric excess determination of chiral α-C-silylated amines and alcohols for the first time.
F. Fortis, J. Picard, B. Barbe and M. Pétraud, Chem. Commun., 1999, 527 DOI: 10.1039/A900491B
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