Carbohydrate-derived 2,3:4,6-diacetonides which are homologated at C-1 by reaction with phenyl acetylide undergo a 6-exo-dig radical cyclization, from a radical located at C-5, to yield highly functionalized cyclohexanes that are correlated with carba-sugars.
A. M. Gómez, G. O. Danelón, E. Moreno, S. Valverde and J. Cristóbal López, Chem. Commun., 1999, 175 DOI: 10.1039/A808848I
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