A convenient large scale procedure for the synthesis of Nicanartine {2,6-di-tert-butyl-4-[5-(3-pyridyl)-4-oxapentyl]phenol}, an antiatherosclerotic compound has been developed, the synthetic route towards the thia-analogue as well as various branched-chain oxa- and thia-derivatives of the parent compound has also been investigated.
O. Pugovičs, V. Kauss, I. Kalvinsh, M. R. Gold and G. Quack, J. Chem. Res. (S), 1998, 430 DOI: 10.1039/A800452H
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