The solid-phase synthesis of asymmetric oligothiophenes on a chloromethylated macroporous resin, using an alternating sequence of bromination and Stille coupling reactions, has been used to afford oligomers up to the pentamer in excellent yield and purity.
P. R. L. Malenfant and J. M. J. Fréchet, Chem. Commun., 1998, 2657 DOI: 10.1039/A807091A
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