Reaction of acylpolysilanes with silylbistriflimides (R3SiNTf2) leads to novel silanols via a pathway involving two 1,2-migrations of Me3Si groups from silicon to carbon and one migration of a R3SiO unit from carbon to silicon; the X-ray structure of one example is reported.
Russell. J. Griffiths, D. S. Yufit, P. G. Steel and M. B. Berry, Chem. Commun., 1998, 2155 DOI: 10.1039/A805966G
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