The tetrahedral indium(I) compound In4[C(SiMe3)3]4 1 reacts with the oxygen donor o-nitrosotoluene to form the extremely hygroscopic In4O4[C(SiMe3)3]4 2 in moderate yield, which exhibits a distorted In4O4 molecular center with normal In–O bond lengths, but short intracage In···In and O···O distances.
W. Uhl and M. Pohlmann, Chem. Commun., 1998, 451 DOI: 10.1039/A706810G
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