Previously unknown tris(nitroxymethyl)methylamine has been synthesised as the free base by nitration of tris(hydroxymethyl)methylamine with nitryl fluoride; by oxidation of tris(nitroxymethyl)methylamine with sodium nitrite in aqueous nitric acid, tris(nitroxymethyl)nitrosomethane, the first representative of aliphatic nitrates containing a nitroso-group, is prepared for the first time.
B. S. Fedorov, M. A. Fadeev and L. T. Eremenko, Mendeleev Commun., 1997, 7, 40 DOI: 10.1070/MC1997v007n01ABEH000683
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