A 1,5-hydrogen migration of a conveniently situated alkoxyl radical affords spironucleosides which possess an unusual orthoamide structure at the anomeric position; X-ray crystallography establishes the configuration of the C-1′ position.
T. Gimisis, C. Chatgilialoglu, T. Gimisis and C. Castellari, Chem. Commun., 1997, 2089 DOI: 10.1039/A705742C
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