Under a one-electron reduction system composed of zinc and an aprotic solvent, alk-4-enyl iodides react with CO and alkenes to give bicyclo[3.3.0]octan-1-ols and bicyclo[3.2.1]octan-1-ols via radical/anionic dual annulations.
S. Tsunoi, M. Tanaka, S. Tsunoi, I. Ryu, S. Yamasaki, N. Sonoda and M. Komatsu, Chem. Commun., 1997, 1889 DOI: 10.1039/A704934J
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