A stereoselective synthesis of trifluoromethylated α-chloro-α,β-unsaturated esters and nitriles by the reaction of fluorinated ylide-anion resulting from nucleophilic addition of organolithium or Grignard reagents to trifluoromethylated phosphoranes with N-chlorosuccinimide is described.
Y. Shen and S. Gao, J. Chem. Soc., Perkin Trans. 1, 1996, 2531 DOI: 10.1039/P19960002531
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