The crystal structure of Li3SbO4 has been determined by analogy with Na3BiO4, and refined by the Rietveld method using X-ray powder diffraction data. It is monoclinic, space group P2/c, a= 5.1579(2), b= 6.0922(3), c= 5.1397(2)Å, β= 108.839(4)°. The structure is an ordered rocksalt type, with distorted MO6 octahedra.
J. M. S. Skakle, M. A. Castellanos R., S. T. Tovar, S. M. Fray and A. R. West, J. Mater. Chem., 1996, 6, 1939 DOI: 10.1039/JM9960601939
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