The structures of two new high nuclearity co-ordination complexes have been determined, a decanuclear cobalt species and an undecanuclear nickel species; the two compounds extend a series of structures based on tricapped-centredtrigonal prisms in displaying respectively no additional capping metal atoms and one capped and one ‘semi-capped’ face.
E. K. Brechin, S. Parsons and R. E. P. Winpenny, J. Chem. Soc., Dalton Trans., 1996, 3745 DOI: 10.1039/DT9960003745
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