Issue 17, 1996

Rapid and mild synthesis of [Re2(CO)10] by reduction of [NH4][ReO4] at atmospheric CO pressure

Abstract

With a view to accessing radiopharmaceuticals based on 186Re and 188Re, a simple, efficient and rapid synthesis at low CO pressure of the key complex [Re2(CO)10] from [NH4][ReO4] using (Me2CHCH2)2 AlH in toluene as reducing agent has been obtained.

Article information

Article type
Paper

J. Chem. Soc., Dalton Trans., 1996, 3611-3612

Rapid and mild synthesis of [Re2(CO)10] by reduction of [NH4][ReO4] at atmospheric CO pressure

S. Top, P. Morel, M. Pankowski and G. Jaouen, J. Chem. Soc., Dalton Trans., 1996, 3611 DOI: 10.1039/DT9960003611

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