SCHEDULED MAINTENANCE
The photochemical cycloaddition of 2-alkoxy-3-cyano-4,6-dimethylpyridine with methacrylonitrile gives a bicyclic azetine, 6-alkoxy-3,5-dicyano-2,5,8-trimethyl-7-azabicyclo-[4.2.0]octa-2,7-diene (45–55% yield) and 3-acetyl-4-amino-1,5-dicyano-2,5-dimethylcyclohexa-1,3-diene (15–17% yield).
M. Sakamoto, T. Sano, M. Takahashi, K. Yamaguchi, T. Fujita and S. Watanabe, Chem. Commun., 1996, 1349 DOI: 10.1039/CC9960001349
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