The ligand-free Pd(OAc)2-catalysed coupling reaction of aryl-, alkenyl- and alkynyl-iodonium tetraflouroborate and iodanes with terminal alkynes proceeds readily in the presence of NaHCO2 in aqueous medium to afford the substituted alkynes in high yields under mild conditions.
S. Kang, H. Lee, S. Jang and P. Ho, Chem. Commun., 1996, 835 DOI: 10.1039/CC9960000835
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