Using a stepwise selective protection–deprotection of tetrathiafulvalene (TTF)-thiolates under high dilution conditions, the first three-dimensional macrobicyclic tetrathiafulvalenophanes are readily prepared.
P. Blanchard, N. Svenstrup and J. Becher, Chem. Commun., 1996, 615 DOI: 10.1039/CC9960000615
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