The diffuse reflectance UV spectra of dehydrated titanium silicalites of MFI structure are consistent with the presence of both open [Ti(OH)(OSi)3] and closed [Ti(OSi)4] tetrahedral titanium sites, the closed sites seem to be the only ones occurring in TiO2–SiO2 silica gel.
D. T. On, L. L. Noc and L. Bonneviot, Chem. Commun., 1996, 299 DOI: 10.1039/CC9960000299
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