Monosodium derivatives of 1,3-bis(diethoxyphosphoryl)-calix[4]arenes undergo O,O-phosphorotropic rearrangement into corresponding 1,2-bis(diethoxyphosphoryl)calix[4]arenes which are useful reagents in the synthesis of asymmetrically substituted calix[4]arenes with AABH-type substitution of the lower rim.
L. N. Markovsky, M. A. Visotsky, V. V. Pirozhenko, V. I. Kalchenko, J. Lipkowski and Y. A. Simonov, Chem. Commun., 1996, 69 DOI: 10.1039/CC9960000069
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