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The use of two different LC–MS techniques, using moving-belt and continuous-flow FAB, has provided complementary means of determining the presence of a diastereomeric impurity within a protected tripeptide pharmaceutical precursor.
E. D. Ramsey, S. D. Lawrence, D. E. Games, M. J. E. Hewlins and M. A. McDowall, Anal. Commun., 1996, 33, 79 DOI: 10.1039/AC9963300079
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