1,3-Bis[tris(trimethylsilyl)methyl]-2,4,5-triselena-1,3-digermabicyclo[1.1.1]pentane 4, obtained by photodeselenation of the corresponding 2,4,5,6-tetraselena-1,3-digermabicyclo[2.1.1]hexane, shows a short Ge ⋯ Ge distance of 2.672 Å; an Se ⋯ Se interaction in 4 is observed by 77Se NMR, X-ray analysis and electronic spectroscopy.
W. Ando, S. Watanabe and N. Choi, J. Chem. Soc., Chem. Commun., 1995, 1683 DOI: 10.1039/C39950001683
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