Treatment of an overcrowded diarylgermylene Tbt(Tip)Ge: 1{Tbt = 2,4,6-tris[bis(trimethylsilyl)methyl]phenyl, Tip = 2,4,6-triisopropylphenyl} with carbon disulfide affords the first germaketenedithioacetal derivative 3 as a stable orange crystalline compound, for which the molecular structure is established by X-ray crystallographic analysis.
N. Tokitoh, K. Kishikawa and R. Okazaki, J. Chem. Soc., Chem. Commun., 1995, 1425 DOI: 10.1039/C39950001425
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