Clear-cut crystallographic evidence of dynamic disorder arising from a reorientational jumping motion of the metal triangle is provided by variable-temperature diffraction experiments on the molecular and crystal structure of [Fe2Os(CO)12].
D. Braga, L. J. Farrugia, F. Grepioni and A. Senior, J. Chem. Soc., Chem. Commun., 1995, 1219 DOI: 10.1039/C39950001219
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