SCHEDULED MAINTENANCE
Electrochemistry is used for the synthesis of [Co(CO)3PBu3]– complex in a methanol–methyl formate medium, which catalyses the alkoxycarbonylation of dichloromethane to dimethyl malonate in up to 75% yield.
P. Suisse, S. Pellegrini, Y. Castanet, A. Mortreux and S. Lecolier, J. Chem. Soc., Chem. Commun., 1995, 847 DOI: 10.1039/C39950000847
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