Quantitative X-ray powder diffractometry was applied to the phase analysis of a mineral specimen containing two sulfur-rich isomorphous mineral phases, beudantite [PbFe3(AsO4)(SO4)(OH)6] and osarizawaite [PbFeAlCu(SO4)2(OH)6], together with goethite (FeOOH) and some hematite (Fe2O3). The application of the Rietveld method was extended to provide elemental as well as phase analysis.
N. Calos, C. H. L. Kennard and L. K. Bekessy, Analyst, 1995, 120, 211 DOI: 10.1039/AN9952000211
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