Issue 24, 1994

Cycloadditions of ketene acetals under microwave irradiation in solvent-free conditions

Abstract

When subjected to microwave irradiation ketene acetals undergo 1,3-dipolar and hetero-Diels–Alder cycloadditions within 5–12 min to give excellent yields of easily purified heterocyclic products. This efficient and rapid synthesis has the advantage of employing milder reaction conditions than those of classical thermal heating.

Article information

Article type
Paper

J. Chem. Soc., Perkin Trans. 1, 1994, 3595-3598

Cycloadditions of ketene acetals under microwave irradiation in solvent-free conditions

A. Díaz-Ortiz, E. Díaz-Barra, A. de la Hoz, P. Prieto and A. Moreno, J. Chem. Soc., Perkin Trans. 1, 1994, 3595 DOI: 10.1039/P19940003595

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