Reaction of [NH4]2[WS4], TIBr and [Bun4N]Br in the solid state produces the mixed-metal sulfur complex [Bun4N][TIWS4]; an X-ray analysis shows that its structure can be described as infinite chains of incomplete double cubane-like [WTI3S7] units interconnected via face-sharing to form a zigzag arrangement.
J. Lang, J. Liu, M. Chen, J. Lu, G. Bian and X. Xin, J. Chem. Soc., Chem. Commun., 1994, 2665 DOI: 10.1039/C39940002665
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