3-Vinylisoxazole is prepared by a sequence involving cycloaddition of acrylonitrile oxide, generated by dehydration of 1-nitropropene, to norbornadiene followed by Diels–Alder cycloreversion of the resulting 2-isoxazoline under flash vacuum pyrolysis conditions.
P. W. Ambler, R. M. Paton and J. M. Tout, J. Chem. Soc., Chem. Commun., 1994, 2661 DOI: 10.1039/C39940002661
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