Leu-Enkephalin, fully labelled with 13C and 15N nuclei in the backbone, is prepared chemically and the corresponding heteronuclear scalar coupling parameters measured from its 13C and 15N NMR spectra.
B. Nyassé, L. Grehn and U. Ragnarsson, J. Chem. Soc., Chem. Commun., 1994, 2005 DOI: 10.1039/C39940002005
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