A new procedure for determining the degree of crystallinity of ZSM-5 using the Raman peak at 382 cm–1 is proposed and is shown to be as accurate as the same parameter determined by X-ray diffraction and more acuate than that determined by infrared absorption measurements.
S. Mintova, B. Mihailova, V. Valtchev and L. Konstantinov, J. Chem. Soc., Chem. Commun., 1994, 1791 DOI: 10.1039/C39940001791
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