A stoichiometric oxide of 3d9 nickel(I), YSr5Ni3O8, has been prepared through the hydrogen reduction of YSr5Ni3O11, resulting in a change from a tetragonal K2NiF4 type structure to an orthorhombic Sr2CuO3 arrangement in which 1/3 of the bridging oxygen atoms are missing from chains of apex-linked nickel oxide square planes.
M. James and J. P. Attfield, J. Chem. Soc., Chem. Commun., 1994, 1185 DOI: 10.1039/C39940001185
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