Single crystal X-ray determination reveals the first example of a mineralomimetic [Cd4(CN)9]– open framework consisting of interconnected tetrahedral and octahedral cadmium centres in the ratio 3 : 1, while solid state 113Cd NMR spectroscopy indicates that some of the bridged cyano groups between the Cd atoms are disordered.
T. Kitazawa, H. Sugisawa, M. Takeda and T. Iwamoto, J. Chem. Soc., Chem. Commun., 1993, 1855 DOI: 10.1039/C39930001855
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