2′-,3′–;4,6;4′,6′-Tri-O-cyclohexylidene-α,α-trehalose 4 is prepared from α,α-trehalose, regioselectively acylated at C-2 with palmitate; after further acylation with palmitate at C-3, deacetalisation gives 2,3-di-O-palmitoyl-α,α-trehalose 2.
P. A. Wallace and D. E. Minnikin, J. Chem. Soc., Chem. Commun., 1993, 1292 DOI: 10.1039/C39930001292
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