The trinuclear complex ion [(NC)(OC)3Re(MoS4)Re(CO)3(CN)]2–12– is reversibly reduced to a MoV containing trianion 13–, which exhibits hypsochromically shifted charge-transfer bands, bathochromically shifted CN, CO and MoS stretching frequencies and an axial EPR signal with g∥ > g⊥.
R. Schäfer, J. Fiedler, M. Moscherosch and W. Kaim, J. Chem. Soc., Chem. Commun., 1993, 896 DOI: 10.1039/C39930000896
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