A facile deoxygenation reaction of phenol and 1,3-dicarbonyl compounds was investigated. Phenols, enolizable 1,3-diketones and 3-ketoesters were converted into the toluene-p-sulfonates which were reduced by a sodium borohydride–nickel chloride system to give the deoxygenated aromatic compounds, alcohols and esters, respectively.
F. Wang, K. Chiba and M. Tada, J. Chem. Soc., Perkin Trans. 1, 1992, 1897 DOI: 10.1039/P19920001897
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