The relatively simple procedure of incorporating doubly labelled 13C–15N into metal cyanide lattices gives a significant simplification of the MAS NMR spectrum, yielding readily interpretable structural information, and the first example of 13C–63,65Cu J coupling constants in the solid state, for NMe4Cu(I)Zn(CN)4.
R. D. Curtis, C. I. Ratcliffe and J. A. Ripmeester, J. Chem. Soc., Chem. Commun., 1992, 1800 DOI: 10.1039/C39920001800
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