The reaction of N,N,N′-tris(trimethylsilyl)formamidine with SeCl2 affords 1,2,3,5-diselenadiazolium chloride, which can be reduced with triphenylantimony to the corresponding diselenadiazolyl radical [HCN2Se2]˙; the solid state structure and conductivity of the dimer [HCN2Se2]2 are reported.
A. W. Cordes, S. H. Glarum, R. C. Haddon, R. Hallford, R. G. Hicks, D. K. Kennepohl, R. T. Oakley, T. T. M. Palstra and S. R. Scott, J. Chem. Soc., Chem. Commun., 1992, 1265 DOI: 10.1039/C39920001265
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