A two-step palladium-catalysed carbonylation, consisting of an oxidative carbonylation of propynyl alcohol, followed by a substitutive carbonylation, leads to E and Z aconitic trimethyl esters in the high yield.
B. Gabriele, M. Costa, G. Salerno and G. P. Chiusoli, J. Chem. Soc., Chem. Commun., 1992, 1007 DOI: 10.1039/C39920001007
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