The interaction of octa(aminopropylsilasequioxane) into metal(IV) hydrogen phosphates [MIV= Zr, Ti, Sn] leads to silica crosslinked materials. The layered structures and the silica framework are retained after thermal processing. Bilayer formation is obtained with tin phosphate.
J. Rozière, D. J. Jones and T. Cassagneau, J. Mater. Chem., 1991, 1, 1081 DOI: 10.1039/JM9910101081
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